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<p>Dear <span class="article__author-link"><a
href="https://pubs.rsc.org/en/results?searchtext=Author%3ARachel%20J.%20Kahan">Rachel</a>,
dear </span><span class="article__author-link"></span><span
class="article__author-link"><a
href="https://pubs.rsc.org/en/results?searchtext=Author%3AF.%20Geoffrey%20N.%20Cloke">Geoffrey</a></span><span
class="article__author-link"></span>,</p>
<p>I'm writing you regarding you article "Activation of carbon
dioxide by new mixed sandwich uranium(iii) complexes" [1] in the
"New Journal of Chemistry". My group is developing methods for
crystallographic data validation, and also maintaining the
Crystallography Open Database [2]. We have received an issue
report from our users that some data in the supplementary CIF of
the article can not be readily interpreted; namely, in the
'c5nj00590f2.cif' file [3], at line 66863, the reflection list
seems to be truncated, with some differently formatted characters
at the end of the text field:</p>
<p>
<blockquote type="cite"><font face="monospace"> -15 -3 -4
28.30 6.20 317-0.60318-0.28871 0.15696-0.29969
0.77632-0.91198<br>
15 -3 4 14.90 6.60 167 0.30325 0.58863-0.18634
0.04361 0.93732-0.80166<br>
15 3 5 0.10 3.60 169 0.34417 0.54801-0.22033
0.36306 0.91588-0.74840<br>
15 -3 5 -7.40 8.00 166 0.27655 0.61563-0.16429
0.02155 0$1 0$1$0$1(0(2? ? 4 4 80 0(0
0&6 0&2 0&2 0&0)0(0 0(0 0"0 0"0
0"0%0"0)0"2 ? !4 4 "10 0$0(0$0(0$0
0(0 0(0$0"4 0"2 0(2%0(6%0"2 0"0 0 0? ? 4
0 00 0(6 0&4 0&0 0 0%0 4%0 4 0 6 0"6
0"6 0&2!0&3 0&5 ? %? !4 0 ! "10
0$4%0"0%0"0!0$0!0$0%0(4 0(2 0$0$0$5$0&7 0&0 0&8??
? 4 0 00 0(4 0"2 0"2 0(2%0(4$0"4 0"6 0$0
0$0 0(0%0(1!0"0? ? !4 0 0 0 "00
0"4$0&0$0&0 0$4 0$2 0"2(0"0%0$0 0$0 0(8!0(1%0&0??
? !4 0 "10 0$4 0 4 0 4$0(0$0(0$0&4
0&2 0"0%0"5(0(4 0(0 0 0?? ? !4 -0 40
0&4 0"0 0"0 0(0!0(1!0 3 0 1 0(0 0(0 0 8!0 8(0"0?? ?
4 0 80 0(1 0"1 0"1 0 0 0 0 0&4 0&6
0(6 0(7 0&4 0&4 0"1 !? !4 0 "20
0"0)0&4)0&0)0&1 0&0 0"2$0"0%0&0 0&0
0&0 0&0 0"0 %? !4 0 "10
0$1)0$1)0$0)0(0)0(0%0&4 0&2 0"2(0"6)0&7 0&0
0"0?? ? !4 -0 1</font></blockquote>
Could it be that the file was damage during or after the upload to
the journal's Web site? If so, maybe you have the original copy of
the data that you could share with us, so that we can update (at
least) the record associated with your publication in the COD [4]?</p>
<p>I would be grateful for your assistance!</p>
<p>Sincerely,<br>
Saulius</p>
<p>Refs.:</p>
<p>[1] <span style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style: normal;
font-variant-caps: normal; font-weight: normal; letter-spacing:
normal; orphans: auto; text-align: start; text-indent: 0px;
text-transform: none; white-space: normal; widows: auto;
word-spacing: 0px; -webkit-text-stroke-width: 0px;
text-decoration: none; display: inline !important; float: none;">Kahan,
R. J.; Cloke, F. G. N.; Roe, S. M. & Nief, F.</span><span
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style: normal;
font-variant-caps: normal; font-weight: normal; letter-spacing:
normal; orphans: auto; text-align: start; text-indent: 0px;
text-transform: none; white-space: normal; widows: auto;
word-spacing: 0px; -webkit-text-stroke-width: 0px;
text-decoration: none; display: inline !important; float: none;">
Activation of carbon dioxide by new mixed sandwich uranium
complexes incorporating cyclooctatetraenyl and pyrrolide,
phospholide, or arsolide ligands.<span
class="Apple-converted-space"> </span></span><em
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-variant-caps: normal; font-weight:
normal; letter-spacing: normal; orphans: auto; text-align:
start; text-indent: 0px; text-transform: none; white-space:
normal; widows: auto; word-spacing: 0px;
-webkit-text-stroke-width: 0px; text-decoration: none;">New
Journal of Chemistry,<span class="Apple-converted-space"> </span></em><span
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style: normal;
font-variant-caps: normal; font-weight: normal; letter-spacing:
normal; orphans: auto; text-align: start; text-indent: 0px;
text-transform: none; white-space: normal; widows: auto;
word-spacing: 0px; -webkit-text-stroke-width: 0px;
text-decoration: none; display: inline !important; float: none;"></span><em
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-variant-caps: normal; font-weight:
normal; letter-spacing: normal; orphans: auto; text-align:
start; text-indent: 0px; text-transform: none; white-space:
normal; widows: auto; word-spacing: 0px;
-webkit-text-stroke-width: 0px; text-decoration: none;">Royal
Society of Chemistry (RSC),<span class="Apple-converted-space"> </span></em><span
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style: normal;
font-variant-caps: normal; font-weight: normal; letter-spacing:
normal; orphans: auto; text-align: start; text-indent: 0px;
text-transform: none; white-space: normal; widows: auto;
word-spacing: 0px; -webkit-text-stroke-width: 0px;
text-decoration: none; display: inline !important; float: none;"></span><b
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-style: normal; font-variant-caps:
normal; letter-spacing: normal; orphans: auto; text-align:
start; text-indent: 0px; text-transform: none; white-space:
normal; widows: auto; word-spacing: 0px;
-webkit-text-stroke-width: 0px; text-decoration: none;">2015</b><i
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-variant-caps: normal; font-weight:
normal; letter-spacing: normal; orphans: auto; text-align:
start; text-indent: 0px; text-transform: none; white-space:
normal; widows: auto; word-spacing: 0px;
-webkit-text-stroke-width: 0px; text-decoration: none;">, 39</i><span
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style: normal;
font-variant-caps: normal; font-weight: normal; letter-spacing:
normal; orphans: auto; text-align: start; text-indent: 0px;
text-transform: none; white-space: normal; widows: auto;
word-spacing: 0px; -webkit-text-stroke-width: 0px;
text-decoration: none; display: inline !important; float: none;">,
7602-7607, DOI: <a class="moz-txt-link-freetext" href="https://doi.org/10.1039/c5nj00590f">https://doi.org/10.1039/c5nj00590f</a> URL:
<a class="moz-txt-link-freetext" href="https://www.rsc.org/suppdata/c5/nj/c5nj00590f/c5nj00590f2.cif">https://www.rsc.org/suppdata/c5/nj/c5nj00590f/c5nj00590f2.cif</a></span></p>
<p><span style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style: normal;
font-variant-caps: normal; font-weight: normal; letter-spacing:
normal; orphans: auto; text-align: start; text-indent: 0px;
text-transform: none; white-space: normal; widows: auto;
word-spacing: 0px; -webkit-text-stroke-width: 0px;
text-decoration: none; display: inline !important; float: none;">[2]
Crystallography Open Database (COD) <b>2023</b>, URL:
<a class="moz-txt-link-freetext" href="https://www.crystallography.net/cod/">https://www.crystallography.net/cod/</a><br>
</span></p>
<p><span style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style: normal;
font-variant-caps: normal; font-weight: normal; letter-spacing:
normal; orphans: auto; text-align: start; text-indent: 0px;
text-transform: none; white-space: normal; widows: auto;
word-spacing: 0px; -webkit-text-stroke-width: 0px;
text-decoration: none; display: inline !important; float: none;">[3]
Article "</span><span style="caret-color: rgb(0, 0, 0); color:
rgb(0, 0, 0); font-family: sans-serif; font-size: medium;
font-style: normal; font-variant-caps: normal; font-weight:
normal; letter-spacing: normal; orphans: auto; text-align:
start; text-indent: 0px; text-transform: none; white-space:
normal; widows: auto; word-spacing: 0px;
-webkit-text-stroke-width: 0px; text-decoration: none; display:
inline !important; float: none;"><span style="caret-color:
rgb(0, 0, 0); color: rgb(0, 0, 0); font-family: sans-serif;
font-size: medium; font-style: normal; font-variant-caps:
normal; font-weight: normal; letter-spacing: normal; orphans:
auto; text-align: start; text-indent: 0px; text-transform:
none; white-space: normal; widows: auto; word-spacing: 0px;
-webkit-text-stroke-width: 0px; text-decoration: none;
display: inline !important; float: none;">Activation of carbon
dioxide by new mixed sandwich uranium complexes ...", DOI</span></span><span
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style: normal;
font-variant-caps: normal; font-weight: normal; letter-spacing:
normal; orphans: auto; text-align: start; text-indent: 0px;
text-transform: none; white-space: normal; widows: auto;
word-spacing: 0px; -webkit-text-stroke-width: 0px;
text-decoration: none; display: inline !important; float: none;"><span
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style:
normal; font-variant-caps: normal; font-weight: normal;
letter-spacing: normal; orphans: auto; text-align: start;
text-indent: 0px; text-transform: none; white-space: normal;
widows: auto; word-spacing: 0px; -webkit-text-stroke-width:
0px; text-decoration: none; display: inline !important; float:
none;"><span style="caret-color: rgb(0, 0, 0); color: rgb(0,
0, 0); font-family: sans-serif; font-size: medium;
font-style: normal; font-variant-caps: normal; font-weight:
normal; letter-spacing: normal; orphans: auto; text-align:
start; text-indent: 0px; text-transform: none; white-space:
normal; widows: auto; word-spacing: 0px;
-webkit-text-stroke-width: 0px; text-decoration: none;
display: inline !important; float: none;">:
10.1039/c5nj00590f</span> – </span>Supplementary files,
Crystal structure data. URL:
<a class="moz-txt-link-freetext" href="https://www.rsc.org/suppdata/c5/nj/c5nj00590f/c5nj00590f2.cif">https://www.rsc.org/suppdata/c5/nj/c5nj00590f/c5nj00590f2.cif</a>
[accessed 2023-02-01T14:40+02:00].</span></p>
<p><span style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style: normal;
font-variant-caps: normal; font-weight: normal; letter-spacing:
normal; orphans: auto; text-align: start; text-indent: 0px;
text-transform: none; white-space: normal; widows: auto;
word-spacing: 0px; -webkit-text-stroke-width: 0px;
text-decoration: none; display: inline !important; float: none;">[4]
COD entry 7054812: structure published in </span><span
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style: normal;
font-variant-caps: normal; font-weight: normal; letter-spacing:
normal; orphans: auto; text-align: start; text-indent: 0px;
text-transform: none; white-space: normal; widows: auto;
word-spacing: 0px; -webkit-text-stroke-width: 0px;
text-decoration: none; display: inline !important; float: none;">
<span style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style:
normal; font-variant-caps: normal; font-weight: normal;
letter-spacing: normal; orphans: auto; text-align: start;
text-indent: 0px; text-transform: none; white-space: normal;
widows: auto; word-spacing: 0px; -webkit-text-stroke-width:
0px; text-decoration: none; display: inline !important; float:
none;">Kahan, R. J.; Cloke, F. G. N.; Roe, S. M. & Nief,
F.</span><span style="caret-color: rgb(0, 0, 0); color: rgb(0,
0, 0); font-family: sans-serif; font-size: medium; font-style:
normal; font-variant-caps: normal; font-weight: normal;
letter-spacing: normal; orphans: auto; text-align: start;
text-indent: 0px; text-transform: none; white-space: normal;
widows: auto; word-spacing: 0px; -webkit-text-stroke-width:
0px; text-decoration: none; display: inline !important; float:
none;"> Activation of carbon dioxide by new mixed sandwich
uranium complexes incorporating cyclooctatetraenyl and
pyrrolide, phospholide, or arsolide ligands.<span
class="Apple-converted-space"> </span></span><em
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-variant-caps: normal;
font-weight: normal; letter-spacing: normal; orphans: auto;
text-align: start; text-indent: 0px; text-transform: none;
white-space: normal; widows: auto; word-spacing: 0px;
-webkit-text-stroke-width: 0px; text-decoration: none;">New
Journal of Chemistry,<span class="Apple-converted-space"> </span></em><span
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style:
normal; font-variant-caps: normal; font-weight: normal;
letter-spacing: normal; orphans: auto; text-align: start;
text-indent: 0px; text-transform: none; white-space: normal;
widows: auto; word-spacing: 0px; -webkit-text-stroke-width:
0px; text-decoration: none; display: inline !important; float:
none;"></span><em style="caret-color: rgb(0, 0, 0); color:
rgb(0, 0, 0); font-family: sans-serif; font-variant-caps:
normal; font-weight: normal; letter-spacing: normal; orphans:
auto; text-align: start; text-indent: 0px; text-transform:
none; white-space: normal; widows: auto; word-spacing: 0px;
-webkit-text-stroke-width: 0px; text-decoration: none;">Royal
Society of Chemistry (RSC),<span class="Apple-converted-space"> </span></em><span
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style:
normal; font-variant-caps: normal; font-weight: normal;
letter-spacing: normal; orphans: auto; text-align: start;
text-indent: 0px; text-transform: none; white-space: normal;
widows: auto; word-spacing: 0px; -webkit-text-stroke-width:
0px; text-decoration: none; display: inline !important; float:
none;"></span><b style="caret-color: rgb(0, 0, 0); color:
rgb(0, 0, 0); font-family: sans-serif; font-style: normal;
font-variant-caps: normal; letter-spacing: normal; orphans:
auto; text-align: start; text-indent: 0px; text-transform:
none; white-space: normal; widows: auto; word-spacing: 0px;
-webkit-text-stroke-width: 0px; text-decoration: none;">2015</b><i
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-variant-caps: normal;
font-weight: normal; letter-spacing: normal; orphans: auto;
text-align: start; text-indent: 0px; text-transform: none;
white-space: normal; widows: auto; word-spacing: 0px;
-webkit-text-stroke-width: 0px; text-decoration: none;">, 39</i><span
style="caret-color: rgb(0, 0, 0); color: rgb(0, 0, 0);
font-family: sans-serif; font-size: medium; font-style:
normal; font-variant-caps: normal; font-weight: normal;
letter-spacing: normal; orphans: auto; text-align: start;
text-indent: 0px; text-transform: none; white-space: normal;
widows: auto; word-spacing: 0px; -webkit-text-stroke-width:
0px; text-decoration: none; display: inline !important; float:
none;">, 7602-7607. <i>Crystallography Open Database, rev. </i></span><b><i>280720</i></b>.
<i>COD Advisory board (eds.)</i>. URL:
<a class="moz-txt-link-freetext" href="http://www.crystallography.net/cod/7054812.html">http://www.crystallography.net/cod/7054812.html</a><br>
</span></p>
<pre class="moz-signature" cols="72">--
Dr. Saulius Gražulis
Vilnius University, Life Science Center, Institute of Biotechnology
Saulėtekio al. 7, LT-10257 Vilnius, Lietuva (Lithuania)
phone (office): (+370-5)-2234353, mobile: (+370-684)-49802, (+370-614)-36366
</pre>
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